Source Publication (e.g., journal title)
JOURNAL OF CHROMATOGRAPHIC SCIENCE
Document Type
Article
Publication Date
2017
DOI
10.1093/chromsci/bmx014
Abstract
A new method of analysis has been developed and validated for the determination of meloxicam in egg whites and yolks. Following a liquid extraction for the whites and a solid phase extraction for the yolks, samples were separated on an XBridge C18 column and quantified using UV detection at 360 nm. The mobile phase was a mixture of water with glacial acetic acid and acetonitrile, with a flow rate of 1 mL/min. The procedure produced a linear curve over the concentration range 5 – 1500 ng/mL with a lower limit of quantification of 5 ng/mL. Intra- and inter-assay variability was 10% or less for both the whites and yolks. The average recovery for whites was 96% and the average recovery in yolks was 97%.
Recommended Citation
Cox, Sherry; Souza, Marcy; Bailey, Joan; White, Molly; and Gordon, Krissten, "Determination of Meloxicam in Egg Whites and Yolks Using Reverse Phase Chromatography" (2017). Faculty Publications and Other Works -- Biomedical and Diagnostic Sciences.
https://trace.tennessee.edu/utk_compmedpubs/115
Submission Type
Post-print