Date of Award
Master of Science
Materials Science and Engineering
Warren Oliver, T. G. Nieh
Measurements of mechanical properties by nanoindentation with triangular pyramidal indenters like the Berkovich rely heavily upon the relationship between the contact stiffness, S, the contact area, A, and the reduced elastic modulus, Er . This relationship is often written in the form: S = 2βEr(A/π)1/2, where βis a constant that depends on the geometry of the indenter. Although the most common values for βused in experimental measurements are 1.000 and 1.034, various theoretical analyses have yielded values as small as 1.00 or as large as 1.2, depending on the assumptions made to model the deformation. Here the most appropriate value of βis explored by performing careful experiments in fused quartz with thin gold coatings applied to the surface to reveal the actual contact area when observed in the scanning electron microscope. Experiments were performed not only with the Berkovich indenter, but with five other three-sided pyramidal indenters with centerline-to-face angles ranging from 35.35o (cube corner) to 85o. Results are discussed as they apply to using the correct value of β in order to correctly determine indenter area functions and obtaining accurate measurements of mechanical properties.
Strader, Jeremy Harper, "An Experimental Evaluation of the Constant β Relating the Contact Stiffness to the Contact Area in Nanoindentation. " Master's Thesis, University of Tennessee, 2005.