Some Quadrivalent Compounds of Rhenium and Technetium Containing Fluorine

The work in this laboratory was begun with the aim of producing pure K₂ReF₆, as a possible intermediate in the preparation of the lower fluorides of rhenium and as a "stand-in" for the preparation of K₂TcF₆. It meant, therefore, the preparation of the white form of K₂ReF₆ which both Weise and Peacock had described as the pure form of the compound.